2,3-二氢-2,2-二甲基苯并呋喃合成路线 (共 32 条)
反应条件
palladium diacetate; potassium carbonate; (S)-p-Tol-BINAP in toluene T=100°C;
参考文献
Palucki, Michael; Wolfe, John P.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1996 , vol. 118, # 42 p. 10333 - 10334
反应条件
caesium carbonate; 2,2,2-trimethylacetic acid; palladium diacetate; PCy3∙HBF4 in 1,3,5-trimethyl-benzene T=135°C; 12 h;
参考文献
Lafrance, Marc; Gorelsky, Serge I.; Fagnou, Keith
Journal of the American Chemical Society, 2007 , vol. 129, # 47 p. 14570 - 14571
反应条件
silver trifluoromethanesulfonate; Ir(III) chloride in 1,2-dichloro-ethane T=60°C; Claisen rearrangement; 4 h;
参考文献
Grant, Virginia H.; Liu, Bing
Tetrahedron Letters, 2005 , vol. 46, # 8 p. 1237 - 1239
反应条件
palladium diacetate; potassium carbonate; (S)-p-Tol-BINAP in toluene T=100°C;
参考文献
Palucki, Michael; Wolfe, John P.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1996 , vol. 118, # 42 p. 10333 - 10334
反应条件
Ni(PCy3)2Cl2; 1,1,3,3-tetramethyldisiloxane; K3PO4 in toluene T=115°C; 15 h; Inert atmosphere;
参考文献
Mesganaw, Tehetena; Fine Nathel, Noah F.; Garg, Neil K.
Organic Letters, 2012 , vol. 14, # 11 p. 2918 - 2921
反应条件
Amberlyst 15 in toluene T=80°C; 24 h;
参考文献
Arduini, Arturo; Pochini, Andrea; Ungaro, Rocco
Synthesis, 1984 , # 11 p. 950 - 953
反应条件
Neutral lead acetate in dichloromethane T=20°C;
参考文献
Birkett, Michael A.; Knight, David W.; Little, Paul B.; Mitchell, Michael B.
Tetrahedron, 2000 , vol. 56, # 7 p. 1013 - 1023
反应条件
N-benzyl-1,4-dihydronicotinamide in methanol T=20°C; 3 h; Irradiation;
参考文献
Kurosawa, Hideo; Okada, Hiroshi; Hattori, Tatsuaki
Tetrahedron Letters, 1981 , vol. 22, # 45 p. 4495 - 4498
反应条件
palladium diacetate; caesium carbonate; PCy3∙HBF4; 2,2,2-trimethylacetic acid in 1,3,5-trimethyl-benzene T=140°C; 16 h; Inert atmosphere;
参考文献
Rousseaux, Sophie; Davi, Michael; Sofack-Kreutzer, Julien; Pierre, Cathleen; Kefalidis, Christos E.; Clot, Eric; Fagnou, Keith; Baudoin, Olivier
Journal of the American Chemical Society, 2010 , vol. 132, # 31 p. 10706 - 10716
反应条件
iodine in dichloromethane 1 h; Ambient temperature;
参考文献
Kim, Kyoung Mahn; Ryu, Eung K.
Heterocycles, 1995 , vol. 41, # 2 p. 219 - 224