2-氯-3-吗啉-1,4-萘醌合成路线 （共 8 条）
反应条件
in acetonitrile T=20°C; 2.5 h;
参考文献
Berezhnaya, V. N.; Shishkina, R. P.; Pavlova, N. V.; Trofimov, A. S.; Eroshkin, V. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 3.2 p. 578 - 583
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 3 p. 657 - 661
反应条件
in water
T=50°C; 0.333333 h;
参考文献
Tandon, Vishnu K.; Maurya, Hardesh K.; Verma, Manoj K.; Kumar, Rohitashw; Shukla, Praveen K.
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 6 p. 2418 - 2426
反应条件
in methanol
0.166667 h; Ambient temperature;
参考文献
Oh, Changsok; Yi, Inwoo; Park, Kyong Pae
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 4 p. 841 - 844
反应条件
in ethanol
2 h; Heating;
参考文献
Avdeenko, A. P.; Yusina, A. L.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 12 p. 1643 - 1645
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 12 p. 1852 - 1854
反应条件
in ethanol
2 h; Heating;
参考文献
Avdeenko, A. P.; Yusina, A. L.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 12 p. 1643 - 1645
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 12 p. 1852 - 1854
反应条件
in ethanol
2 h; Heating;
参考文献
Avdeenko, A. P.; Yusina, A. L.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 12 p. 1643 - 1645
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 12 p. 1852 - 1854
反应条件
in methanol-d4
0.166667 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Oh, Changsok; Yi, Inwoo; Park, Kyong Pae
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 4 p. 841 - 844
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; 2 h;
2: With hydrogenchloride in tetrahydrofuran; water
参考文献
TRANSITIONS OPTICAL, INC.
Patent: EP994871 B1, 2006 ;
Location in patent: Page/Page column 14 ;
