吲哚并[3,2-b]咔唑合成路线 (共 11 条)
反应条件
sulfuric acid in methanol 0.0833333 h; Heating;
参考文献
Archiv der Pharmazie, , vol. 320, # 3 p. 280 - 282
反应条件
sulfuric acid in acetic acid T=0 - 45°C;
参考文献
EP2371828 A1, ;
Page/Page column 36 ;
反应条件
hydrogenchloride in tetrahydrofuran Heating;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 9, # 4 p. 955 - 960
反应条件
sulfuric acid; acetic acid T=0 - 110°C; Fischer cyclization;
参考文献
Tetrahedron, , vol. 59, # 8 p. 1265 - 1275
反应条件
triethyl phosphite in various solvent(s) 48 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1237 - 1239
反应条件
1: 61 percent / Na2CO3 / tetrakis(triphenylphosphino)palladium(0) / H2O; toluene / 24 h / Heating 2: 35 percent / P(OEt)3 / various solvent(s) / 48 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1237 - 1239
反应条件
hydrogenchloride in ethanol; water Cyclization; hydrolysis; 7 h; Heating; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 55, # 19 p. 6243 - 6260
反应条件
1: H2SO4 2: 2 percent / methanol View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 35, # 5 p. 561 - 569
反应条件
polyphosphoric acid trimethysilyl ester Fischer cyclization;
参考文献
Tetrahedron, , vol. 59, # 8 p. 1265 - 1275
反应条件
in methanol Condensation;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 35, # 5 p. 561 - 569