2-(4-氯苯基)-1-苯乙酮合成路线 (共 67 条)
反应条件
(i) NaNO2, aq. acid, (ii) /BRN= 2042489/, CuCl, acetone; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 1926 - 1931
参考文献
Journal of the American Chemical Society, , vol. 77, p. 3070,3073
反应条件
T=150°C; im Einschmelzrohr;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 67, p. 378
反应条件
sodium hydride in tetrahydrofuran 4 h; Inert atmosphereRefluxSchlenk technique;
参考文献
Yang, Dongmei; Zhou, Yuhan; Xue, Na; Qu, Jingping
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4171 - 4176
反应条件
potassium hydroxide; hydrazine hydrate in diethylene glycol
参考文献
Robinson,G.E.; Vernon,J.M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1276 - 1281
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; bis(1,2-diphenylphosphino)benzene in chlorobenzene 6 h; Inert atmosphereReflux;
参考文献
Li, Guangzhe; Arisawa, Mieko; Yamaguchi, Masahiko
Chemical Communications, 2014 , vol. 50, # 33 p. 4328 - 4330
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide T=90°C; 24 h;
参考文献
Qi, Chaorong; Jiang, Huanfeng; Huang, Liangbin; Chen, Zhengwang; Chen, Huoji
Synthesis, 2011 , # 3 art. no. F17110SS, p. 387 - 396
反应条件
potassium permanganate; thionyl chloride; aluminium trichloride in pyridine; dichloromethane; water; benzene
参考文献
Rohm and Haas Company
Patent: US4009022 A1, 1977 ;
反应条件
RhH(CO)(PPh3)3; bis(1,2-diphenylphosphino)benzene in 1,3-dimethyl-imidazolidin-2-one T=150°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 14 p. 3804 - 3807
反应条件
RhH(CO)(PPh3)3; bis(1,2-diphenylphosphino)benzene in 1,3-dimethyl-imidazolidin-2-one T=150°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 14 p. 3804 - 3807