2-(4-氯苯基)-1-苯乙酮合成路线 （共 67 条）
反应条件
sodium periodate in methanol
参考文献
Synthesis, , p. 268 - 269
反应条件
1: 62 percent / CH2Cl2 / 40 - 42 °C 2: 64 percent / KOH / ethanol / Heating View Scheme
参考文献
Synlett, , # 14 p. 2189 - 2192
反应条件
1: Et3N / tetrahydrofuran / 0 deg C, then 2 h, room t. 2: LDA(3 equiv.) / tetrahydrofuran / 4 h / Ambient temperature; addition, -70 deg C 3: tetrahydrofuran / cooling, then 1 h, room t. 4: Et3N / tetrahydrofuran / 0 deg C, then 2 h, room t. 5: 78 percent / LDA / tetrahydrofuran / 4 h / 0 °C / adding, -70 deg C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2496 - 2502
反应条件
1: triethylamine / CHCl3 2: 61 percent / NaH / tetrahydrofuran / 14 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 22, p. 123 - 126
反应条件
hydrogenchloride; iron in ethanol Heating;
参考文献
Bulletin de la Societe Chimique de France, , vol. <II>, p. 362 - 365
反应条件
1: LDA / tetrahydrofuran / 2 h / 0 °C / adding, -70 deg C 2: tetrahydrofuran / cooling, then 1 h, room t. 3: Et3N / tetrahydrofuran / 0 deg C, then 2 h, room t. 4: 78 percent / LDA / tetrahydrofuran / 4 h / 0 °C / adding, -70 deg C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2496 - 2502
反应条件
1: LDA(3 equiv.) / tetrahydrofuran / 4 h / Ambient temperature; addition, -70 deg C 2: tetrahydrofuran / cooling, then 1 h, room t. 3: Et3N / tetrahydrofuran / 0 deg C, then 2 h, room t. 4: 78 percent / LDA / tetrahydrofuran / 4 h / 0 °C / adding, -70 deg C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2496 - 2502
反应条件
1: N2O4 / CCl4 2: Fe, AcOH 3: aq. HCl / Heating View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. <II>, p. 362 - 365
反应条件
hydrogenchloride T=150°C; im Einschmelzrohr;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 67, p. 379
反应条件
1: boron trifluoride etherate / CH2Cl2 / 2 h / cooling 2: 92 percent / ethylene diamine / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 37, # 5 p. 661 - 665
