2-(4-氯苯基)-1-苯乙酮合成路线 (共 67 条)
反应条件
diethyl ether; hydrogen Behandeln des Reaktionsgemisches mit Eis und Schwefelsaeure;
参考文献
Journal of the American Chemical Society, , vol. 56, p. 682
Journal of the American Chemical Society, , vol. 55, p. 1618,1619
反应条件
in tetrahydrofuran; water T=50°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 41, # 52 p. 10327 - 10331
反应条件
trimethylsilyl iodide in chloroform 3 h;
参考文献
Synthetic Communications, , vol. 16, # 4 p. 377 - 386
反应条件
copper; zinc; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran room temp., 5 h; 60 deg C, 18 h;
参考文献
Tetrahedron Letters, , vol. 24, # 36 p. 3869 - 3872
反应条件
in benzene Irradiation;
参考文献
Synthesis, , p. 268 - 269
反应条件
1: tetrahydrofuran / cooling, then 1 h, room t. 2: Et3N / tetrahydrofuran / 0 deg C, then 2 h, room t. 3: 78 percent / LDA / tetrahydrofuran / 4 h / 0 °C / adding, -70 deg C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2496 - 2502
反应条件
1: LDA(3 equiv.) / tetrahydrofuran / 3 h / Ambient temperature; addition, -70 deg C 2: tetrahydrofuran / cooling, then 1 h, room t. 3: Et3N / tetrahydrofuran / 0 deg C, then 2 h, room t. 4: 78 percent / LDA / tetrahydrofuran / 4 h / 0 °C / adding, -70 deg C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2496 - 2502
反应条件
1: NaOH / dimethylsulfoxide 2: NaBH4 / methanol 3: aq. NaIO4 / methanol View Scheme
参考文献
Synthesis, , p. 268 - 269
反应条件
1: NaOH / dimethylsulfoxide 2: NaBH4 / methanol 3: aq. NaIO4 / methanol View Scheme
参考文献
Synthesis, , p. 268 - 269
反应条件
water; palladium diacetate; potassium hydrogencarbonate; tri-cyclo-hexyl-phosphine T=100°C; Suzuki coupling; P=7500.75 Torr; 20 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 788 - 792