1: With AlCl3, aluminium chloride in dichloromethane
T=0 - 20°C; Friedel-Crafts Acylation; 27 h;
2: With hydrogenchloride in dichloromethane; water
Cooling with ice;
参考文献
Okazaki, Takao; Adachi, Taisuke; Kitagawa, Toshikazu
Bulletin of the Chemical Society of Japan, 2013 , vol. 86, # 4 p. 464 - 471
Campbell et al.
Journal of the Chemical Society, 1951 , p. 1404
Full Text Show Details
Campbell; Easton
Journal of the Chemical Society, 1949 , p. 340,344
Campbell et al.
Journal of the Chemical Society, 1951 , p. 1404
Full Text Show Details
Campbell; Easton
Journal of the Chemical Society, 1949 , p. 340,344
diethyl ether; ethanol; Ethoxymagnesiummalonsaeure-diethylester
weiteres Reagens: Benzol; Erhitzen des Reaktionsprodukts mit Essigsaeure und wss. H2SO4;
参考文献
Campbell; Keir
Journal of the Chemical Society, 1955 , p. 1233,1237