反应条件
1: 5-Bromo-2,4(1H,3H)-pyrimidinedione With chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane in 1,2-dichloro-ethane
Inert atmosphereReflux;
2: methyl iodide With iodine in 1,2-dichloro-ethane
12 h; Inert atmosphereReflux;
参考文献
Shelke, Sandip A.; Sigurdsson, Snorri Th.
Nucleic Acids Research, 2012 , vol. 40, # 8 p. 3732 - 3740