N-(4-氰基苯基)甲酰胺合成路线 （共 10 条）
反应条件
oxygen; Mn(OAc)3•2H2O in toluene
T=90°C; P=760.051 Torr; 12 h;
参考文献
Zhang, Chun; Xu, Zejun; Shen, Tao; Wu, Guolin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2012 , vol. 14, # 9 p. 2362 - 2365
反应条件
oxygen; Mn(OAc)3•2H2O in chloroform; toluene
T=90°C; P=760.051 Torr; 12 h;
参考文献
Zhang, Chun; Xu, Zejun; Shen, Tao; Wu, Guolin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2012 , vol. 14, # 9 p. 2362 - 2365
反应条件
oxygen; Mn(OAc)3•2H2O in toluene
T=90°C; P=760.051 Torr; 12 h;
参考文献
Zhang, Chun; Xu, Zejun; Shen, Tao; Wu, Guolin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2012 , vol. 14, # 9 p. 2362 - 2365
参考文献
Nagarajan; Ho; DuBois
Synthetic Communications, 1992 , vol. 22, # 8 p. 1191 - 1198
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Kamijo; Jin; Yamamoto
Journal of the American Chemical Society, 2001 , vol. 123, # 38 p. 9453 - 9454
反应条件
1: 84 percent / p-TsOH; Si(OEt)4 / toluene / Heating
2: H2 / Pd/C / ethanol / 2 h / 1551.44 Torr
3: Heating
4: liq. NH3 / 80 - 90 °C
View Scheme
参考文献
Ostrowski; Wolniewicz
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 6 p. 705 - 713
反应条件
1: H2 / Pd/C / ethanol / 2 h / 1551.44 Torr
2: Heating
3: liq. NH3 / 80 - 90 °C
View Scheme
参考文献
Ostrowski; Wolniewicz
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 6 p. 705 - 713
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl
T=150°C; 24 h; Inert atmosphere;
参考文献
Romero; Harrak; Basset; Orue; Pujol
Tetrahedron, 2009 , vol. 65, # 10 p. 1951 - 1956
反应条件
in water
24 h; Reflux;
参考文献
Kaboudin, Babak; Khodamorady, Minoo
Synlett, 2010 , # 19 p. 2905 - 2907
反应条件
diisopropylamine; trichlorophosphate in dichloromethane
1.) 0 deg C, 1 h, 2.) r.t., 14 h;
参考文献
Deschenaux, Robert; Masoni, Claudio; Stoeckli-Evans, Helen; Vaucher, Sebastien; Ketterer, Juergen; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1994 , # 7 p. 1051 - 1060
