2-氯-N-(2-羟基乙基)-乙酰胺合成路线 (共 7 条)
反应条件
unter vermindertem Druck und Erwaermen des Reaktionsprodukts mit Pyridin;
参考文献
Epstein; Harris
Patent: US2290173 , 1940 ;
反应条件
sodium hydride in tetrahydrofuran T=20 - 60°C; 6 h; Inert atmosphereCooling with ice;
参考文献
JAPAN TOBACCO INC.
Patent: US2011/306599 A1, 2011 ;
Location in patent: Page/Page column 35 ;
反应条件
thionyl chloride; chloroform T=40°C;
参考文献
Jones; Wilson
Journal of the Chemical Society, 1949 , p. 550
反应条件
in chloroform
T=20°C;
参考文献
Hirata; Watanabe; Miura; Ijichi; Fukasawa; Sakakibara
Bioscience, biotechnology, and biochemistry, 2000 , vol. 64, # 10 p. 2047 - 2052
反应条件
Lipozyme RM 1 M in acetone
T=55°C; 48 h; Enzymatic reaction;
参考文献
Rustoy, Eduardo M.; Baldessari, Alicia
European Journal of Organic Chemistry, 2005 , # 21 p. 4628 - 4632
反应条件
sodium hydroxide in water
pH=10; 0.5 h;
参考文献
Barge, Alessandro; Tei, Lorenzo; Upadhyaya, Dharita; Fedeli, Franco; Beltrami, Lorena; Stefania, Rachele; Aime, Silvio; Cravotto, Giancarlo
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 7 p. 1176 - 1184
参考文献
McCormick, Joan E.; McElhinney, R. Stanley
Journal of Chemical Research, Miniprint, 1983 , # 7 p. 1736 - 1800