2,4,6-三硝基二甲苯合成路线 （共 32 条）
反应条件
1: chromium trioxide; concentrated sulfuric acid / 80 - 90 °C 2: water View Scheme
参考文献
Giua
Gazzetta Chimica Italiana, 1922 , vol. 52 I, p. 186
反应条件
(NH4)2S Behandeln des Diamins in Alkohol mit nitrosen Daempfen;
参考文献
v. Pechmann; Nold
Chemische Berichte, 1898 , vol. 31, p. 559
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Miolati; Lotti
Gazzetta Chimica Italiana, 1897 , vol. 27 I, p. 295
反应条件
1: ammonium sulfide / Behandeln des Diamins in Alkohol mit nitrosen Daempfen 2: zinc dust; aqueous alcohol; ammonium chloride View Scheme
参考文献
v. Pechmann; Nold
Chemische Berichte, 1898 , vol. 31, p. 559
反应条件
sulfuric acid; nitric acid
T=110°C; 3 h;
参考文献
Liu, Ju Na; Ban, Shu Rong; Xie, Hong Yu; Li, Qing Shan
Chinese Chemical Letters, 2012 , vol. 23, # 8 p. 907 - 910
反应条件
sodium acetate; acetic acid
T=35 - 45°C; Electrolysis;
参考文献
Fieser; Clapp; Daudt
Journal of the American Chemical Society, 1942 , vol. 64, p. 2052,2059
反应条件
nitrogen(IV) oxide; ozone; methanesulfonic acid in dichloromethane
T=-10 - 0°C; 9 h;
参考文献
Suzuki, Hitomi; Murashima, Takashi; Kozai, Iku; Mori, Tadashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 14 p. 1591 - 1598
反应条件
nitric acid
T=20°C; 1 h;
参考文献
Havlik, Martin; Kral, Vladimir; Dolensky, Bohumil
Organic Letters, 2006 , vol. 8, # 21 p. 4867 - 4870
反应条件
1: lead (IV)-acetate; glacial acetic acid
2: lead (IV)-acetate; glacial acetic acid
View Scheme
参考文献
Fieser; Clapp; Daudt
Journal of the American Chemical Society, 1942 , vol. 64, p. 2052,2059
反应条件
sulfuric acid; nitric acid
参考文献
Knoevenagel
Justus Liebigs Annalen der Chemie, 1896 , vol. 289, p. 143
Justus Liebigs Annalen der Chemie, 1897 , vol. 297, p. 119,160, 175
反应条件
sulfuric acid; nitric acid
参考文献
Blanksma
Recueil des Travaux Chimiques des Pays-Bas, 1906 , vol. 25, p. 175
Recueil des Travaux Chimiques des Pays-Bas, 1909 , vol. 28, p. 93
