1,1,2,2-四苯基乙烷合成路线 (共 396 条)
反应条件
hydrogen; aluminum oxide; K6SiCu(H2O)W11O39
T=300°C; Catalytic hydrogenation; P=17480 Torr; 3.33333 h; Title compound not separated from byproducts;
参考文献
Kogan, Vladimir; Aizenshtat, Zeev; Neumann, Ronny
Angewandte Chemie - International Edition, 1999 , vol. 38, # 22 p. 3331 - 3334
反应条件
sodium formate; ((n-Bu)4N)2S2O8 in N,N-dimethyl-formamide
T=60°C; Barton-McCombie deoxygenation; 1 h;
参考文献
Hee, Sock Park; Hee, Yoon Lee; Yong, Hae Kim
Organic Letters, 2005 , vol. 7, # 15 p. 3187 - 3190
反应条件
acetic acid; mercury; lithium chloride; zinc
2 h; Heating;
参考文献
Vona, Maria Luisa Di; Rosnati, Vittorio
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4269 - 4273
反应条件
titanium in tetrahydrofuran
20 h; Heating;
参考文献
Dams, Rudy; Malinowski, Marek; Giese, Herman J.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 3 p. 112 - 114
反应条件
lanthanum; chloro-trimethyl-silane; iodine; copper(l) iodide; water in acetonitrile
T=82°C; 1 h;
参考文献
Nishino, Toshiki; Nishiyama, Yutaka; Sonoda, Noboru
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 3 p. 635 - 641
反应条件
cyclohexa-1,4-diene; potassium tert-butylate in dimethyl sulfoxide
T=20°C; 3 h; Schlenk techniqueInert atmosphereIrradiationGreen chemistry; Quantum yield;
参考文献
Oksdath-Mansilla, Gabriela; Argueello, Juan E.; Penenory, Alicia B.
Tetrahedron Letters, 2013 , vol. 54, # 12 p. 1515 - 1518
反应条件
sodium; lithium in tetrahydrofuran
T=20°C; 14.5 h; Inert atmosphere; regioselective reaction;
参考文献
Pittalis, Mario; Azzena, Ugo; Pisano, Luisa
Tetrahedron, 2013 , vol. 69, # 1 p. 207 - 211
反应条件
in tetrahydrofuran
T=-70°C; 0.0833333 h; further solvent; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takagi, Masato; NOjima, Masamoto; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4676 - 4684
参考文献
Wang; Cohen
Journal of the American Chemical Society, 1957 , vol. 79, p. 1924,1928
Full Text Show Details
Cohen; Wang
Journal of the American Chemical Society, 1955 , vol. 77, p. 2457,2460
反应条件
lithium perchlorate in tetrahydrofuran
T=0°C; 3 h; electrochemical anion oxidation;
参考文献
Bank, Shelton; Gernon, Michael
Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5105 - 5111