2,4-二氯喹啉-3-甲酸乙酯合成路线 （共 14 条）
反应条件
copper; acetic acid 5 h; Heating;
参考文献
Ukrainets, I. V.; Taran, S. G.; Gorokhova, O. V.; Marusenko, N. A.; Kovalenko, S. N.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 2 p. 167 - 175
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 2 p. 195 - 203
反应条件
hydrogenchloride 3 h; Heating;
参考文献
Ukrainets, I. V.; Taran, S. G.; Gorokhova, O. V.; Marusenko, N. A.; Kovalenko, S. N.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 2 p. 167 - 175
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 2 p. 195 - 203
反应条件
1: 96 percent / AcOH, AcONa / 10 h / Heating 2: 67 percent / Zn, gl. AcOH / 5 h / Heating View Scheme
参考文献
Ukrainets, I. V.; Taran, S. G.; Gorokhova, O. V.; Marusenko, N. A.; Kovalenko, S. N.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 2 p. 167 - 175
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 2 p. 195 - 203
反应条件
potassium hydroxide 2 h; Heating;
参考文献
Ukrainets, I. V.; Taran, S. G.; Gorokhova, O. V.; Marusenko, N. A.; Kovalenko, S. N.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 2 p. 167 - 175
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 2 p. 195 - 203
反应条件
triethylamine; trichlorophosphate
T=60°C; 2 h;
参考文献
Stadlbauer, Wolfgang; Prattes, Susanne; Fiala, Werner
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 3 p. 627 - 636
反应条件
trichlorophosphate
T=105°C; 120 h;
参考文献
Ukrainets; Bereznyakova; Davidenko; Slobodzian
Chemistry of Heterocyclic Compounds, 2009 , vol. 45, # 8 p. 952 - 956
反应条件
trichlorophosphate
T=100°C; 0.0833333 h;
参考文献
Ukrainets; Gorokhova; Sidorenko
Chemistry of Heterocyclic Compounds, 2005 , vol. 41, # 8 p. 1019 - 1021
反应条件
trichlorophosphate
a) heating, 3 h, b) RT, 5 d;
参考文献
Ukrainets, I. V.; Taran, S. G.; Gorokhova, O. V.; Marusenko, N. A.; Kovalenko, S. N.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 2 p. 167 - 175
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 2 p. 195 - 203
反应条件
1: sodium ethanolate / ethanol / 14.5 h / 20 - 140 °C
2: trichlorophosphate / 6 h / 110 °C
View Scheme
参考文献
Ohashi, Tomohiro; Oguro, Yuya; Tanaka, Toshio; Shiokawa, Zenyu; Shibata, Sachio; Sato, Yoshihiko; Yamakawa, Hiroko; Hattori, Harumi; Yamamoto, Yukiko; Kondo, Shigeru; Miyamoto, Maki; Tojo, Hideaki; Baba, Atsuo; Sasaki, Satoshi
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 18 p. 5496 - 5506
反应条件
1: 40 percent / MeONa / methanol / 10 h / 140 - 150 °C
2: 98 percent / POCl3, Et3N / 2 h / 60 °C
View Scheme
参考文献
Stadlbauer, Wolfgang; Prattes, Susanne; Fiala, Werner
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 3 p. 627 - 636
