N-叔丁基-3-氯丙烷-1-磺酰胺合成路线 （共 5 条）
反应条件
in tetrahydrofuran T=20°C; 24 h;
参考文献
Hewawasam, Piyasena; Ding, Min; Sun, Li-Qiang; Scola, Paul Michael
Patent: US2007/10455 A1, 2007 ;
Location in patent: Page/Page column 26 ;
反应条件
1: N-(tert-butyl)-3-chloropropane-1-sulfonamide With n-butyllithium in tetrahydrofuran; hexane T=-69 - 20°C; 4.33333 h; 2: methyl iodide in tetrahydrofuran; hexane T=-65 - 50°C; 4.66667 h;
参考文献
Bristol-Myers Squibb Company; Zheng, Zhizhen Barbara; D'Andrea, Stanley
Patent: US2013/102589 A1, 2013 ;
Location in patent: Paragraph 0072; 0073 ;
反应条件
1: N-(tert-butyl)-3-chloropropane-1-sulfonamide With n-butyllithium in tetrahydrofuran; hexane
2: allyl bromide in tetrahydrofuran; hexane
参考文献
Li, Jianqing; Smith, Daniel; Wong, Henry S.; Campbell, Jeffrey A.; Meanwell, Nicholas A.; Scola, Paul M.
Synlett, 2006 , # 5 p. 725 - 728
反应条件
1: N-(tert-butyl)-3-chloropropane-1-sulfonamide With n-butyllithium in tetrahydrofuran; hexane
2: benzoic acid methyl ester in tetrahydrofuran; hexane
参考文献
Li, Jianqing; Smith, Daniel; Wong, Henry S.; Campbell, Jeffrey A.; Meanwell, Nicholas A.; Scola, Paul M.
Synlett, 2006 , # 5 p. 725 - 728
反应条件
1: N-(tert-butyl)-3-chloropropane-1-sulfonamide With n-butyllithium in tetrahydrofuran; hexane
2: benzyl bromide in tetrahydrofuran; hexane
参考文献
Li, Jianqing; Smith, Daniel; Wong, Henry S.; Campbell, Jeffrey A.; Meanwell, Nicholas A.; Scola, Paul M.
Synlett, 2006 , # 5 p. 725 - 728
