N-乙酰基-2-(甲硫基)苯胺合成路线 （共 10 条）
反应条件
trichlorophosphate T=130°C;
参考文献
Chemische Berichte, , vol. 48, p. 1247
参考文献
Chemische Berichte, , vol. 48, p. 1247
反应条件
sodium perborate in acetic acid
参考文献
McKillop, Alexander; Tarbin, Jonathan A.
Tetrahedron, 1987 , vol. 43, # 8 p. 1753 - 1758
反应条件
triethylamine in chloroform
T=20 - 90°C; 2 - 3 h; Product distribution / selectivity;
参考文献
Anadys Pharmaceuticals, Inc.
Patent: US2008/292588 A1, 2008 ;
Location in patent: Page/Page column 48; 52 ;
反应条件
1: 0.0166667 h; Microwave irradiation;
2: With water in diethyl ether
参考文献
Saez, Rebeca; Dolores Otero; Batanero, Belen; Barba, Fructuoso
Journal of Chemical Research, 2008 , # 9 p. 492 - 494
反应条件
in benzene
T=90°C; 1 h;
参考文献
Reichardt, Christian; Erfurt, Hans-Peter; Harms, Klaus
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 5 p. 1081 - 1092
反应条件
1: 52 percent / aq. NaOH / 2 h / Heating
2: 68 percent / benzene / 1 h / 90 °C
View Scheme
参考文献
Reichardt, Christian; Erfurt, Hans-Peter; Harms, Klaus
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 5 p. 1081 - 1092
反应条件
1: zinc; concentrated hydrochloric acid
2: sodium acetate
View Scheme
参考文献
Zincke; Siebert
Chemische Berichte, 1915 , vol. 48, p. 1247
反应条件
1: 53 percent / 30percent H2O2 / acetic acid / 240 h / Heating
2: 86 percent / 5N aq NaOH / ethanol / 8 h / Heating
View Scheme
参考文献
Zincke; Siebert
Chemische Berichte, 1915 , vol. 48, p. 1247
反应条件
trichlorophosphate
T=20 - 130°C; 3 h;
参考文献
Reichardt, Christian; Erfurt, Hans-Peter; Harms, Klaus
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 5 p. 1081 - 1092
