1,3-二(4-甲氧基苯基)异苯并呋喃合成路线 (共 15 条)
反应条件
1: in tetrahydrofuran
T=-40 - 0°C; 1 h;
2: With trifluoroacetic acid in tetrahydrofuran
T=25°C; 1.5 h;
参考文献
Hamura, Toshiyuki; Nakayama, Ryosuke
Chemistry Letters, 2013 , vol. 42, # 9 p. 1013 - 1015
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Benderradji, Farah; Nechab, Malek; Einhorn, Cathy; Einhorn, Jacques
Synlett, 2006 , # 13 p. 2035 - 2038
参考文献
Blicke; Weinkauff
Journal of the American Chemical Society, 1932 , vol. 54, p. 1446,1451
反应条件
PPA
T=110°C; 0.166667 h;
参考文献
Oida, Tatsuo; Tanimoto, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Synthesis, 1980 , # 2 p. 131 - 133
反应条件
1: bromine / 180 - 200 °C / Leiten von Luft durch das Reaktionsgemisch
2: silver nitrate; ethanol
3: diethyl ether; benzene / Erwaermen des Reaktionsprodukts in Aceton mit wss. Salzsaeure
View Scheme
参考文献
Blicke; Patelski
Journal of the American Chemical Society, 1936 , vol. 58, p. 559,561
反应条件
1: silver nitrate; ethanol
2: diethyl ether; benzene / Erwaermen des Reaktionsprodukts in Aceton mit wss. Salzsaeure
View Scheme
参考文献
Blicke; Patelski
Journal of the American Chemical Society, 1936 , vol. 58, p. 559,561
反应条件
diethyl ether; benzene
参考文献
Blicke; Patelski
Journal of the American Chemical Society, 1936 , vol. 58, p. 273,274
反应条件
thionyl chloride; benzene
Erhitzen der Reaktionsloesung unter Durchleiten von Wasserdampf;
参考文献
Blicke; Swisher
Journal of the American Chemical Society, 1934 , vol. 56, p. 1406
反应条件
diethyl ether; benzene
Erwaermen des Reaktionsprodukts in Aceton mit wss. Salzsaeure;
参考文献
Blicke; Patelski
Journal of the American Chemical Society, 1936 , vol. 58, p. 559,561
反应条件
1: 92 percent / diethyl ether / 2 h / Ambient temperature
2: 30 percent / polyphosphoric acid / 0.17 h / 110 °C
View Scheme
参考文献
Oida, Tatsuo; Tanimoto, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Synthesis, 1980 , # 2 p. 131 - 133