2-酞酰亚胺基-3-甲基丁酸合成路线 (共 12 条)
反应条件
1: thionyl chloride / tetrahydrofuran / 2.5 h / Inert atmosphere; Reflux
2: 4-(N,N-dimethlyamino)pyridine; triethylamine / tetrahydrofuran / 18 h / 20 °C
3: hydrazine hydrate / ethanol / 18 h / 20 °C
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参考文献
Wixey, James S.; Ward, Benjamin D.
Chemical Communications, 2011 , vol. 47, # 19 p. 5449 - 5451
反应条件
1: dicyclohexylcarbodiimide / Erwaermen des Reaktionsprodukts mit wss.Salzsaeure in Aceton
2: N2H4+H2O; ethanol
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参考文献
Shankman; Schvo
Journal of the American Chemical Society, 1958 , vol. 80, p. 1164,1167