2-酞酰亚胺基-3-甲基丁酸合成路线 （共 12 条）
参考文献
Angewandte Chemie, , vol. 104, # 1 p. 97 - 99
反应条件
potassium carbonate in acetonitrile T=20°C; 3 h;
参考文献
The Journal of organic chemistry, , vol. 67, # 11 p. 3764 - 3768
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 11 p. 4177 - 4187
反应条件
sodium carbonate in ethyl acetate
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 475 - 483
反应条件
1: 98 percent / DCC / 1,2-dimethoxy-ethane / 6 h / 0 °C 2: 89 percent / aq. K2CO3 / acetonitrile / 3 h / 20 °C View Scheme
参考文献
The Journal of organic chemistry, , vol. 67, # 11 p. 3764 - 3768
反应条件
2,6-di-tert-butyl-pyridine; 2-hydroxy-1,3-dimethylbenzene; C32H12BF24(1-)*C44H30N2O2P(1+) in toluene T=20°C; 2 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 132, # 35 p. 12240 - 12242
反应条件
acetic acid in methanol Resolution of racemate;
参考文献
Asian Journal of Chemistry, , vol. 22, # 2 p. 1582 - 1586
反应条件
1: dicyclohexylcarbodiimide; tetrahydrofuran / Behandeln des Reaktionsprodukts mit wss.Natronlauge in Dioxan 2: N2H4+H2O; ethanol View Scheme
参考文献
Obata; Mizutani
Bulletin of the Agricultural Chemical Society of Japan, 1959 , vol. 23, p. 121,123
反应条件
in acetone 3 h; Irradiation;
参考文献
Sato, Yasuhiko; Nakai, Hideo; Mizoguchi, Tomishige; Kawanishi, Masazumi; Hatanaka, Yasumaru; Kanaoka, Yuichi
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1263 - 1270
反应条件
1: thionyl chloride / tetrahydrofuran / 2.5 h / Inert atmosphere; Reflux
2: 4-(N,N-dimethlyamino)pyridine; triethylamine / tetrahydrofuran / 18 h / 20 °C
3: hydrazine hydrate / ethanol / 18 h / 20 °C
View Scheme
参考文献
Wixey, James S.; Ward, Benjamin D.
Chemical Communications, 2011 , vol. 47, # 19 p. 5449 - 5451
