Parkinson, Elizabeth I.; Jason Hatfield; Tsurkan, Lyudmila; Hyatt, Janice L.; Edwards, Carol C.; Hicks, Latorya D.; Yan, Bing; Potter, Philip M.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 15 p. 4635 - 4643
1: 1-bromo-hexane With magnesium in tetrahydrofuran
T=-78°C;
2: With copper(I) bromide; lithium bromide in tetrahydrofuran
T=-100 - -75°C;
3: oxalyl dichloride in tetrahydrofuran
T=-95 - -90°C; 1 h; Further stages.;
参考文献
Kenning, Don D.; Mitchell, Kari A.; Calhoun, Tessa R.; Funfar, Melanie R.; Sattler, Daniel J.; Rasmussen, Seth C.
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 9073 - 9076
