2-氯-4'-羟基苯乙酮合成路线 （共 35 条）
反应条件
in tetrahydrofuran T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1373 - 1380
反应条件
in tetrahydrofuran T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1373 - 1380
反应条件
1: 40 percent / triethylamine / acetonitrile / 3 h / Heating 2: 75 percent / 2 h / 100 °C 3: hydrogen chloride; methanol / ethyl acetate / 24 h / 20 °C 4: potassium hydroxide / methanol; H2O / 1 h / 0 - 4 °C View Scheme
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
反应条件
in methanol 24 h; Ambient temperature;
参考文献
Gurjar, M.K.; Joshi, Shreerang V; Sastry, B.S.; Rao, A V Rama
Synthetic Communications, 1990 , vol. 20, # 22 p. 3489 - 3496
反应条件
diethyl ether; n-Butyl nitrite Einleiten von Chlorwasserstoff;
参考文献
Levin; Hartung
Journal of Organic Chemistry, 1942 , vol. 7, p. 408,412
反应条件
1: 50 percent / Et3N / acetonitrile / 3 h / Heating 2: acetonitrile / 0.25 h / Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 121, # 24 p. 5625 - 5632
反应条件
methyloxirane in water; acetonitrile 4 h; Irradiation;
参考文献
Tetrahedron, , vol. 53, # 49 p. 16789 - 16794
反应条件
1: 50 percent / Et3N / acetonitrile / 3 h / Heating 2: H2O / acetonitrile / Ambient temperature; Irradiation; other p-hydroxyphenacyl esters; also in absence of H2O; var. pH's; kinetic isotope effect View Scheme
参考文献
Zhang, Kai; Corrie, John E. T.; Munasinghe, V. Ranjit N.; Wan, Peter
Journal of the American Chemical Society, 1999 , vol. 121, # 24 p. 5625 - 5632
反应条件
sodium azide; ethanol
参考文献
Fries; Saftien
Chemische Berichte, 1926 , vol. 59, p. 1251
反应条件
methanol; diethyl ether
参考文献
Hayashi
Acta Phytochimica, 1933 , vol. 7, p. 117,138
Acta Phytochimica, 1934 , vol. 8, p. 65,93
