2-氯-4'-羟基苯乙酮合成路线 (共 35 条)
反应条件
aluminium trichloride in various solvent(s) T=70°C; 5 h;
参考文献
Gurjar, M.K.; Joshi, Shreerang V; Sastry, B.S.; Rao, A V Rama
Synthetic Communications, 1990 , vol. 20, # 22 p. 3489 - 3496
反应条件
sodium hydroxide in methanol; water T=0 - 20°C; 0.5 h;
参考文献
Chen, Jian
Patent: US2005/250944 A1, 2005 ;
Location in patent: Page/Page column 19 ;
US 20050250944 A1
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate in methanol; 1,2-dichloro-ethane 10 h; Heating;
参考文献
Kajigaeshi, Shoji; Kakinami, Takaaki; Moriwaki, Masayuki; Fujisaki, Shizuo; Maeno, Kimihiro; Okamoto, Tsuyoshi
Synthesis, 1988 , # 7 p. 545 - 546
反应条件
aluminium trichloride; Petroleum ether
参考文献
Journal of Organic Chemistry, , vol. 5, p. 54,57
Journal of the American Pharmaceutical Association (1912-1977), , vol. 35, p. 306,308
Journal of Organic Chemistry, , vol. 6, p. 384,388, 390
反应条件
beryllium(II) chloride T=130 - 140°C;
参考文献
Chemische Berichte, , vol. 72, p. 1414,1424
反应条件
aluminium trichloride T=120°C;
参考文献
Chemische Berichte, , vol. 43, p. 215
Chemische Berichte, , vol. 44, p. 114
反应条件
aluminium trichloride in n-heptane 2.5 h; Heating;
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
反应条件
1: AlCl3 / heptane / 1.5 h / 35 °C 2: 9.5 g / AlCl3 / heptane / 2.5 h / Heating View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 49, # 13 p. 1151 - 1162
反应条件
1: HCl / methanol / 10 °C 2: 110 °C View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 73, p. 579 - 584
反应条件
aluminium trichloride; tetrachloroethane, 1,1,2,2-
参考文献
DE935363 , ;
US2838570 , ;