2,2-二甲氧基乙基巯基甲基苯合成路线 （共 8 条）
反应条件
sulfuric acid in toluene Rearrangement; 72 h; Heating;
参考文献
Journal of the Chinese Chemical Society, , vol. 46, # 4 p. 601 - 605
反应条件
sulfuric acid in toluene T=20°C; Rearrangement; 120 h;
参考文献
Journal of the Chinese Chemical Society, , vol. 46, # 4 p. 601 - 605
反应条件
sodium hydride in tetrahydrofuran
T=0 - 20°C;
参考文献
Sugimura, Hideyuki; Kusakabe, Kousuke
Synlett, 2013 , vol. 24, # 1 p. 69 - 72
反应条件
1: phenylmethanethiol With sodium hydride in tetrahydrofuran
Metallation; 2 h; Heating;
2: chloroacetaldehyde dimethyl acetal in tetrahydrofuran
Condensation; 48 h; Heating;
参考文献
Ong, Chi Wi; Yen, Sin Fei; Chou, Yi Meen
Journal of the Chinese Chemical Society, 1999 , vol. 46, # 4 p. 601 - 605
参考文献
Parham et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2065,2069
反应条件
sulfuric acid in water
T=60°C;
参考文献
Zhdanko, Alexander G.; Gulevich, Anton V.; Nenajdenko, Valentine G.
Tetrahedron, 2009 , vol. 65, # 24 p. 4692 - 4702
反应条件
sulfuric acid in toluene
T=20°C; Rearrangement; 120 h;
参考文献
Ong, Chi Wi; Yen, Sin Fei; Chou, Yi Meen
Journal of the Chinese Chemical Society, 1999 , vol. 46, # 4 p. 601 - 605
反应条件
1: aqueous H2SO4
View Scheme
参考文献
Gawron; Glaid
Journal of the American Chemical Society, 1949 , vol. 71, p. 3232
