双(2-氯乙基)-(2-氯乙基)膦酸酯合成路线 （共 22 条）
反应条件
1,1-dibromomethane T=170°C; Michaelis-Arbuzov reaction; 1 h; Microwave irradiationNeat (no solvent);
参考文献
Jansa, Petr; Holy, Antonin; Dracinsky, Martin; Baszczynski, Ondrej; Cesnek, Michal; Janeba, Zlatko
Green Chemistry, 2011 , vol. 13, # 4 p. 882 - 888
反应条件
hydrogenchloride T=120°C; P=3800 Torr; 16 h; Product distribution; Further Variations:PressuresTemperatures;
参考文献
Ilia, Gheorghe; Caprita, Adrian; Iliescu, Smaranda; Popa, Adriana; Pascariu, Aurelia; Bora, Alina; Dehelean, Gheorghe
Revue Roumaine de Chimie, 2004 , vol. 49, # 6 p. 501 - 506
反应条件
hydrogenchloride T=150°C; P=3750.38 Torr; High pressure;
参考文献
Asian Journal of Chemistry, , vol. 25, # 11 p. 6463 - 6464
反应条件
hydrogenchloride T=120°C; P=3800 Torr; 16 h; Product distribution; Further Variations:PressuresTemperatures;
参考文献
Revue Roumaine de Chimie, , vol. 49, # 6 p. 501 - 506
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 515,519
Chem.Abstr., , p. 7243
反应条件
hydrogenchloride T=120°C; P=3800 Torr; 16 h; Product distribution; Further Variations:PressuresTemperatures;
参考文献
Ilia, Gheorghe; Caprita, Adrian; Iliescu, Smaranda; Popa, Adriana; Pascariu, Aurelia; Bora, Alina; Dehelean, Gheorghe
Revue Roumaine de Chimie, 2004 , vol. 49, # 6 p. 501 - 506
反应条件
thionyl chloride; N,N-dimethyl-formamide 70 h; Heating;
参考文献
Maier, Ludwig
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 47, p. 465 - 470
反应条件
thionyl chloride; N,N-dimethyl-formamide 1) 22 h, reflux, 2) 10 h, 135 deg C (bomb tube);
参考文献
Maier, Ludwig
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 47, p. 465 - 470
参考文献
Kabatschnik; Rossiiskaja
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1946 , p. 515,519
Chem.Abstr., 1948 , p. 7243
反应条件
air T=220 - 230°C; PyrolysisMicrowave irradiation;
参考文献
Zotov; Tuzhikov; Khokhlova
Russian Journal of Applied Chemistry, 2012 , vol. 85, # 4 p. 639 - 643
