二乙基[2-(异丁基氨基)-2-氧代乙基]膦酸酯合成路线 （共 3 条）
反应条件
in diethyl ether
T=0 - 20°C; 5 h;
参考文献
TSUMURA and CO.; Aoki, Katsuyuki
Patent: US2013/245303 A1, 2013 ;
Location in patent: Paragraph 0084; 0085; 0086 ;
反应条件
1: oxalyl dichloride / dichloromethane / 16 h / 20 °C / |Inert atmosphere
2: diethyl ether / 5 h / 0 - 20 °C
View Scheme
参考文献
TSUMURA and CO.; Aoki, Katsuyuki
Patent: US2013/245303 A1, 2013 ;
参考文献
Landor; Odyek
Journal of the Chemical Society. Perkin transactions 1, 1977 , vol. 2, p. 93 - 95
