1: 98 percent / lithium aluminum hydride / diethyl ether / 0.67 h / 0 °C
2: dichloroacetic acid / 72 h / Ambient temperature
3: hexamethylphosphoric triamide / tetrahydrofuran; hexane / Ambient temperature
4: ethanolic HCl / Ambient temperature
5: 76 percent / H2NCH2CH2CH2NHK, H2NCH2CH2CH2NH2 / tetrahydrofuran
View Scheme
参考文献
Okada, Shuji; Matsuda, Hiro; Otsuka, Masaaki; Kikuchi, Naoto; Hayamizu, Kikuko; et al.
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 2 p. 455 - 461