3-羟基-4-甲氧基-2-硝基苯甲醛合成路线 （共 5 条）
反应条件
nitronium tetrafluoroborate in dichloromethane T=-20°C; 24 h; Inert atmosphere;
参考文献
Turkman, Nashaat; Shavrin, Aleksander; Ivanov, Roman A.; Rabinovich, Brian; Volgin, Andrei; Gelovani, Juri G.; Alauddin, Mian M.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 18 p. 5698 - 5707
反应条件
sulfuric acid; nitric acid in water; acetic acid
参考文献
Japan Tobacco Inc.
Patent: US6017919 A1, 2000 ;
反应条件
AcONO2; silica gel in chloroform T=-20 - 20°C; Nitration;
参考文献
Tetrahedron, , vol. 55, # 22 p. 6733 - 6738
反应条件
ethanol; sodium carbonate
参考文献
Hey; Lobo
Journal of the Chemical Society, 1954 , p. 2246,2255
Full Text Show Details
Tomita; Kikkawa
Yakugaku Zasshi, 1957 , vol. 77, p. 195,199
Chem.Abstr., 1957 , p. 9648
反应条件
caesium carbonate; sodium iodide in N,N-dimethyl-formamide
T=20 - 80°C; 25 h; Inert atmosphere;
参考文献
Turkman, Nashaat; Shavrin, Aleksander; Ivanov, Roman A.; Rabinovich, Brian; Volgin, Andrei; Gelovani, Juri G.; Alauddin, Mian M.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 18 p. 5698 - 5707
