3-乙酰基-2(1H)-吡啶酮合成路线 （共 9 条）
反应条件
in acetic anhydride 64 h; Reflux;
参考文献
WO2012/112743 A1, ;
Page/Page column 74 ;
反应条件
dihydrogen peroxide in hydrogenchloride 20 h; Heating;
参考文献
Trecourt, Francois; Marsais, Francis; Guengoer, Timur; Queguiner, Guy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2409 - 2415
反应条件
AcOF; water 1.) -40 deg C, CHCl3, 2.) 50 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Heterocycles, , vol. 28, # 1 p. 249 - 258
反应条件
1: dihydrogen peroxide / methyltrioxorhenium (VII) / acetic acid / 16 h / 20 °C 2: acetic anhydride / 64 h / Reflux View Scheme
反应条件
1: 1) butyllithium, di-isopropylamine / 1) THF, hexane, 0 deg C, 1 h 2) THF, -70 deg C, 3 h 2: 95 percent / chromic anhydride / acetone / 3 h / Ambient temperature 3: 72 percent / 3percentH2O2 / aq. HCl / 20 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 2409 - 2415
反应条件
1: 95 percent / chromic anhydride / acetone / 3 h / Ambient temperature 2: 72 percent / 3percentH2O2 / aq. HCl / 20 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 2409 - 2415
反应条件
trifluoroacetic acid
参考文献
Journal of Organic Chemistry, , vol. 58, # 1 p. 95 - 99
反应条件
1: 93 percent / CuI, PdCl2(PPh3), triethylamine / 2 h / Heating 2: trifluoroacetic acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 1 p. 95 - 99
参考文献
Tetrahedron, , vol. 57, # 42 p. 8841 - 8850
