N-芴甲氧羰基DMNB-L-丝氨酸合成路线 （共 4 条）
反应条件
4-methyl-morpholine; tetrakis(triphenylphosphine) palladium(0); acetic acid in chloroform
T=20°C; 4 h;
参考文献
Veldhuyzen, Willem F.; Nguyen, Quan; McMaster, Gary; Lawrence, David S.
Journal of the American Chemical Society, 2003 , vol. 125, # 44 p. 13358 - 13359
反应条件
1: 85 percent / K2CO3; Et3N / CH2Cl2 / 24 h / 20 °C
2: CF3SO3H / CH2Cl2 / 20 °C
3: Pd(Ph3P)4; N-methylmorpholine; acetic acid / CHCl3 / 4 h / 20 °C
View Scheme
参考文献
Veldhuyzen, Willem F.; Nguyen, Quan; McMaster, Gary; Lawrence, David S.
Journal of the American Chemical Society, 2003 , vol. 125, # 44 p. 13358 - 13359
反应条件
1: tricaprylmethylammonium chloride; aq. NaHCO3 / CH2Cl2 / 24 h / 20 °C
2: CF3SO3H / CH2Cl2 / 20 °C
3: Pd(Ph3P)4; N-methylmorpholine; acetic acid / CHCl3 / 4 h / 20 °C
View Scheme
参考文献
Veldhuyzen, Willem F.; Nguyen, Quan; McMaster, Gary; Lawrence, David S.
Journal of the American Chemical Society, 2003 , vol. 125, # 44 p. 13358 - 13359
反应条件
1: CF3SO3H / CH2Cl2 / 20 °C
2: Pd(Ph3P)4; N-methylmorpholine; acetic acid / CHCl3 / 4 h / 20 °C
View Scheme
参考文献
Veldhuyzen, Willem F.; Nguyen, Quan; McMaster, Gary; Lawrence, David S.
Journal of the American Chemical Society, 2003 , vol. 125, # 44 p. 13358 - 13359
