2-(2-丙烯基)-苯并噻唑合成路线 （共 9 条）
反应条件
1: cyclobenzothiazole With (TMP)2Zn*2MgCl2*2LiCl in tetrahydrofuran
T=25°C; 0.5 h;
2: allyl bromide With CuCN*2LiCl in tetrahydrofuran
T=0°C; 0.5 h; Further stages.;
参考文献
Wunderlich, Stefan H.; Knochel, Paul
Angewandte Chemie - International Edition, 2007 , vol. 46, # 40 p. 7685 - 7688
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in tetrahydrofuran
T=100°C; 3 h;
参考文献
Itoh, Takashi; Hasegawa, Hiroshi; Nagata, Kazuhiro; Ohsawa, Akio
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1319 - 1325
反应条件
potassium carbonate; potassium hexacyanoferrate(III) in 1,4-dioxane
3 h; Heating;
参考文献
Itoh, Takashi; Hasegawa, Hiroshi; Nagata, Kazuhiro; Ohsawa, Akio
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1319 - 1325
反应条件
in tetrahydrofuran
T=-70°C; 0.25 h;
参考文献
Boga, Carla; Forlani, Luciano; Todesco, Paolo E.
Gazzetta Chimica Italiana, 1997 , vol. 127, # 4 p. 197 - 200
反应条件
in dichloromethane
T=0°C;
参考文献
Florio, Saverio; Epifani, Erbana; Ingrosso, Giovanni
Tetrahedron, 1984 , vol. 40, # 21 p. 4527 - 4534
反应条件
in dichloromethane
T=0°C;
参考文献
Florio, Saverio; Epifani, Erbana; Ingrosso, Giovanni
Tetrahedron, 1984 , vol. 40, # 21 p. 4527 - 4534
反应条件
in dichloromethane
T=0°C;
参考文献
Florio, Saverio; Epifani, Erbana; Ingrosso, Giovanni
Tetrahedron, 1984 , vol. 40, # 21 p. 4527 - 4534
反应条件
1: 80 percent / Et3N, air / dimethylsulfoxide / 12 h / Ambient temperature
2: 40 percent / tetrahydrofuran / 0.25 h / -70 °C
View Scheme
参考文献
Boga, Carla; Forlani, Luciano; Todesco, Paolo E.
Gazzetta Chimica Italiana, 1997 , vol. 127, # 4 p. 197 - 200
参考文献
Florio, Saverio; Epifani, Erbana; Ingrosso, Giovanni
Tetrahedron, 1984 , vol. 40, # 21 p. 4527 - 4534
