反应条件
1: 85 percent / DIPEA; DMAP / CH2Cl2 / 5 h / 20 °C 2: 85 percent / NaN3; NH4Cl / methanol / 40 h / Heating 3: 72 percent / m-chloroperbenzoic acid / CH2Cl2 / 20 °C 4: 82 percent / Yb(OTf)3; Et3N; NaN3 / molecular sieves 4 Angstroem / toluene / 96 h / 80 °C 5: 100 percent / HCl / methanol / 20 °C 6: 95 percent / H2 / Pd/C / methanol / 14 h / 2250.18 Torr View Scheme
参考文献
Busscher, Guuske F.; Groothuys, Stan; De Gelder, Rene; Rutjes, Floris P. J. T.; Van Delft, Floris L.
Journal of Organic Chemistry, 2004 , vol. 69, # 13 p. 4477 - 4481
