N-(3,4-二甲氧基苯乙基)乙酰胺合成路线 (共 31 条)
参考文献
Judeh, Zaher M.A.; Ching, Chi Bun; Bu, Jie; McCluskey, Adam
Tetrahedron Letters, 2002 , vol. 43, # 29 p. 5089 - 5091
参考文献
Spaeth; Polgar
Monatshefte fuer Chemie, 1929 , vol. 51, p. 199
反应条件
(i) NaNO2, Ac2O, AcOH, (ii) benzene, (heating); Multistep reaction;
参考文献
Fujii,T. et al.
Chemical and Pharmaceutical Bulletin, 1960 , vol. 8, p. 266 - 269
反应条件
1: 86 percent / AlCl3 / nitrobenzene / 2.5 h / 35 °C 2: 99 percent / 1N HCl / 18 h / Heating View Scheme
参考文献
Orito, Kazuhiko; Matsuzaki, Tsutomu; Suginome, Hiroshi; Rodrigo, Russel
Heterocycles, 1988 , vol. 27, # 10 p. 2403 - 2412
反应条件
1: 88 percent / AlCl3 / nitrobenzene / 2.5 h / 35 °C 2: 93 percent / 1N HCl / 18 h / Heating View Scheme
参考文献
Orito, Kazuhiko; Matsuzaki, Tsutomu; Suginome, Hiroshi; Rodrigo, Russel
Heterocycles, 1988 , vol. 27, # 10 p. 2403 - 2412
反应条件
1: 87 percent / POCl3 2: 75 percent / phenethole / 10percent Pd/C / 1 h / Heating 3: 25 percent / SeO2 4: 50 percent / NH2OH View Scheme
参考文献
Postaire, E.; Martinez, D.; Viel, C.; Chastagnier, M.; Hamon, M.
Bulletin de la Societe Chimique de France, 1988 , # 6 p. 982 - 988
反应条件
boron tribromide in dichloromethane T=0 - 20°C; 20 h;
参考文献
Fong, Hugo K.H.; Copp, Brent R.
Marine Drugs, 2013 , vol. 11, # 2 p. 274 - 299
反应条件
1: (i) NaNO2, Ac2O, AcOH, (ii) benzene, (heating) 2: KOH / methanol / Heating View Scheme
参考文献
Fujii,T. et al.
Chemical and Pharmaceutical Bulletin, 1960 , vol. 8, p. 266 - 269
反应条件
1: trichlorophosphate / toluene / 2 h / 20 - 111 °C / Inert atmosphere 2: formic acid; N-[(1R,2R)-2-(dimethylamino)-1,2-diphenylethyl]-4-methylbenzenesulfonamide benzene ruthenium chloride / isopropyl alcohol / 19 h / 30 °C / 760.05 Torr / Inert atmosphere View Scheme
参考文献
Soni, Rina; Cheung, Fung Kei; Clarkson, Guy C.; Martins, Jose E. D.; Graham, Mark A.; Wills, Martin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3290 - 3294
反应条件
1: 84 percent / LiAlH4 / tetrahydrofuran / 6 h / Heating 2: 1.) n-BuLi, 2.) n-BuLi View Scheme
参考文献
Lete, Esther; Collado, M. Isabel; Sotomayor, Nuria; Vicente, Teresa; Villa, Maria-Jesus
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 6 p. 1751 - 1758