2-氨基-5-甲氧基苯硫酚合成路线 （共 29 条）
反应条件
1: With potassium hydroxide; water 24 h; Heating / reflux; 2: With hydrogenchloride; water; acetic acid pH=6;
参考文献
GE HEALTHCARE LIMITED; GE HEALTHCARE AS
Patent: WO2007/20400 A1, 2007 ;
Location in patent: Page/Page column 21-22 ;
参考文献
Glaxo Wellcome Inc.
Patent: US5998400 A1, 1999 ;
反应条件
DL-threo-1,4-dimercapto-2,3-butanediol in N,N-dimethyl-formamide
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 6 p. 1532 - 1536
反应条件
2: alkali hydrolysis View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, # 1-12 p. 189 - 190
反应条件
1: 64 percent / H2O / 4 h / Heating 2: 35 percent / bromine / CHCl3 / 2 h 3: 51 percent / aq. sodium hydroxide / 48 h / Heating View Scheme
参考文献
Biological and Pharmaceutical Bulletin, , vol. 25, # 3 p. 335 - 341
反应条件
1: With ammonium hydroxide 2: With potassium hydroxide in water Reflux; 3: With acetic acid in water T=20°C;
参考文献
Research on Chemical Intermediates, , vol. 37, # 8 p. 1103 - 1111
反应条件
1: 35 percent / bromine / CHCl3 / 2 h 2: 51 percent / aq. sodium hydroxide / 48 h / Heating View Scheme
参考文献
Biological and Pharmaceutical Bulletin, , vol. 25, # 3 p. 335 - 341
参考文献
Yakugaku Zasshi, , vol. 71, p. 41,43
Chem.Abstr., , p. 7109
参考文献
Canadian Journal of Chemistry, , vol. 43, p. 2610 - 2612
反应条件
oxygen in dimethyl sulfoxide; chlorobenzene T=140°C; P=760.051 Torr; 16 h; Sealed tube;
参考文献
Liao, Yunfeng; Qi, Hongrui; Chen, Shanping; Jiang, Pengcheng; Zhou, Wang; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 23 p. 6004 - 6007
