5-溴-1,3-二氯-2-碘苯合成路线 （共 5 条）
反应条件
sodium methylate in methanol; dimethyl sulfoxide T=323.2°C; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1593 - 1598
反应条件
potassium iodide; sulfuric acid; sodium thiosulfate; sodium nitrite in ice-water
参考文献
JAPAN POLYPROPYLENE CORPORATION
Patent: US2005/70426 A1, 2005 ;
反应条件
sulfuric acid; acetic acid; potassium iodide; sodium nitrite
1.)0-5 deg C; 2.)heated; Yield given. Multistep reaction;
参考文献
Bolton, Roger; Moore, Clive; Sandall, John P.B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1593 - 1598
反应条件
1.1: bromine; hydrochloric acid
2.1: sodium nitrite; HCl / H2O
2.2: potassium iodide / H2O
View Scheme
参考文献
Prasad, M. Arun; Sangaranarayanan
Tetrahedron, 2004 , vol. 60, # 48 p. 10967 - 10972
反应条件
n-butyllithium; trimethylsilyl trifluoromethanesulfonate in diethyl ether; hexane; water
参考文献
JAPAN POLYPROPYLENE CORPORATION
Patent: US2005/70426 A1, 2005 ;
