反应条件
1: 94 percent / SnCl4 / CH2Cl2 / 1.) 0 deg C, 10 min, 2.) 20 deg C, 3 h
2: 80 percent / Et3N, 4-(dimethylamino)pyridine / CH2Cl2 / 48 h / 20 °C
3: 1.) sodium α-(dimethylamino)naphthalenide / 1.) benzene, HMPA, 30 s, 2.) 30 min
View Scheme
参考文献
Ghosh, Subrata; Pardo, Simon N.; Salomon, Robert G.
Journal of Organic Chemistry, 1982 , vol. 47, # 24 p. 4692 - 4702
