1-苯基-1,3-丙烷二醇二乙酸酯合成路线 （共 18 条）
反应条件
p-Nitrobenzene sulphonamide; iodine in 1,2-dichloro-ethane
T=60°C; 2 h; Inert atmosphere;
参考文献
Baba, Haruka; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4303 - 4307
反应条件
cobalt(II) chloride in acetonitrile
T=80°C; 3 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
cobalt(II) chloride in acetonitrile
T=80°C; 3 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
bis(acetylacetonato) palladium; silver(I) acetate
T=60°C; Inert atmosphereSealed vial;
参考文献
Satterfield, Andrew D.; Kubota, Asako; Sanford, Melanie S.
Organic Letters, 2011 , vol. 13, # 5 p. 1076 - 1079
反应条件
1: 56 percent / Ag2CO3 / Pd(OAc)2, PPh3 / dimethylformamide / 24 h / 60 °C
2: 95 percent / H2 / 5percent Pd-C / methanol
3: HCl
View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Tetrahedron Letters, 1992 , vol. 33, # 45 p. 6845 - 6848
反应条件
1: 95 percent / H2 / 5percent Pd-C / methanol
2: HCl
View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Tetrahedron Letters, 1992 , vol. 33, # 45 p. 6845 - 6848
反应条件
1: 60 percent / BuLi / diethyl ether / 8 h / Ambient temperature
2: 2 g / methylsulphinylcarbanion / dimethylsulfoxide / 10 °C
View Scheme
参考文献
Medlik-Balan, A.; Klein, J.
Tetrahedron, 1980 , vol. 36, # 2 p. 299 - 304
反应条件
1: 2 g / methylsulphinylcarbanion / dimethylsulfoxide / 10 °C
View Scheme
参考文献
Medlik-Balan, A.; Klein, J.
Tetrahedron, 1980 , vol. 36, # 2 p. 299 - 304
反应条件
iodine in dichloromethane
参考文献
Atkinson,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1977 , p. 230 - 238
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Tetrahedron Letters, 1992 , vol. 33, # 45 p. 6845 - 6848
