1,2-丙二醇-1-醋酸酯合成路线 (共 15 条)
反应条件
T=525°C; an Glasoberflaechen;
参考文献
Wyandotte Chem.Corp.
Patent: US2415378 , 1944 ;
反应条件
yttria-stabilized zirconia in acetonitrile
T=40°C; 10 h;
参考文献
Kumar; Pandey; Bodas; Dongare
Synlett, 2001 , # 2 p. 206 - 209
反应条件
hydrogen; triethylamine in hexane
T=23°C; P=3800.26 Torr; 10 h; Autoclave;
参考文献
Kawamorita, Soichiro; Hamasaka, Go; Ohmiya, Hirohisa; Hara, Kenji; Fukuoka, Atsushi; Sawamura, Masaya
Organic Letters, 2008 , vol. 10, # 20 p. 4697 - 4700
反应条件
tetra-n-butylammonium acetate in acetonitrile
T=40°C; 6 h; regioselective reaction;
参考文献
Zhou, Yixuan; Ramstroem, Olof; Dong, Hai
Chemical Communications, 2012 , vol. 48, # 43 p. 5370 - 5372
反应条件
tetrachloromethane; CuCl2·2H2O; Cr(acetylacetone)3; water
T=130°C; 6 h; Sealed tube;
参考文献
Khusnutdinov; Oshnyakova; Shchadneva
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 10 p. 1428 - 1432
Zhurnal Organicheskoi Khimii, 2013 , vol. 49, # 10 p. 1451 - 1455,5
反应条件
tetra-n-butylammonium acetate in acetonitrile
T=40°C; regioselective reaction;
参考文献
Zhou, Yixuan; Rahm, Martin; Wu, Bin; Zhang, Xiaoling; Ren, Bo; Dong, Hai
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11618 - 11622
反应条件
pyridine
T=37°C; 10 h; pronase E (proteases from Streptomyces griseus); Title compound not separated from byproducts;
参考文献
Bhattacharya, A; Ali, E
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 12 p. 898 - 899
反应条件
water
T=130°C; 6 h; Autoclave; regioselective reaction;
参考文献
Khusnutdinov; Schadneva; Oshnyakova; Dzhemilev
Petroleum Chemistry, 2009 , vol. 49, # 4 p. 331 - 338
反应条件
Ea; variation of reactant concentrations, solvents, temperature; effect of the amount of alkali-metal acetate catalyst; Rate constantMechanismThermodynamic data;
参考文献
Szakacs, Sandor; Goeboeloes, Sandor; Nagy, Ferenc
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 417 - 420
反应条件
bis(acetonitrile)chloronitropalladium(II)
T=25°C; 2 h; various catalysts, times, O2 atmosphere with 18O containing complex; further products; Product distribution;
参考文献
Mares, Frank; Diamond, Steven E.; Regina, Francis J.; Solar, Jeffrey P.
Journal of the American Chemical Society, 1985 , vol. 107, # 12 p. 3545 - 3552