2,5-二甲基-1,5-己二烯合成路线 （共 92 条）
反应条件
1: With magnesium in diethyl ether 2: With boron trifluoride in diethyl ether
参考文献
Sattely, Elizabeth S.; Alexander Cortez; Moebius, David C.; Schrock, Richard R.; Hoveyda, Amir H.
Journal of the American Chemical Society, 2005 , vol. 127, # 23 p. 8526 - 8533
反应条件
TCA in dichloromethane T=12°C; Irradiation;
参考文献
Tsuji, Takashi; Miura, Toshimasa; Sugiura, Kenichi; Matsumoto, Yoshiyuki; Nishida, Shinya
Journal of the American Chemical Society, 1993 , vol. 115, # 2 p. 482 - 493
反应条件
manganese; copper dichloride in water 16 h; Ambient temperature;
参考文献
Ma, Jihai; Chan, Tak-Hang
Tetrahedron Letters, 1998 , vol. 39, # 17 p. 2499 - 2502
反应条件
dihydrogen peroxide T=530°C;
参考文献
Journal of the American Chemical Society, , vol. 79, p. 3997,3999
反应条件
methanol; tetracarbonylnickel(0) T=50°C;
反应条件
carbon monoxide in tetrahydrofuran
参考文献
Journal of the American Chemical Society, , vol. 90, p. 2416 - 2417
反应条件
T=374 - 383°C; P=760 Torr; (pyrolysis);
参考文献
Journal of the American Chemical Society, , vol. 83, p. 3457 - 3461
反应条件
1: 2-methylphenylmagnesium chloride With zinc(II) chloride in tetrahydrofuran T=0 - 20°C; 2: methallylsulfonyl chloride With Pd0(tris(tert-butyl)phosphine)2 in tetrahydrofuran Negishi reaction; Heating;
参考文献
Tetrahedron Letters, , vol. 47, # 20 p. 3345 - 3348
反应条件
1: 72 percent / oxygen / cyclohexane-d12 / 1.5 h / 4 °C 2: 100 percent Spectr. / cyclohexane-d12 / 3 h / 80 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 24 p. 7782 - 7795
反应条件
1: 87 percent / KOH / methanol; H2O / 6 h / 160 °C 2: 72 percent / oxygen / cyclohexane-d12 / 1.5 h / 4 °C 3: 100 percent Spectr. / cyclohexane-d12 / 3 h / 80 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 24 p. 7782 - 7795
