3,4-二氢-6,7-二甲氧基-1-甲基异喹啉盐酸盐合成路线 (共 6 条)
反应条件
potassium carbonate; sodium chloride in dichloromethane Inert atmosphere;
参考文献
Soni, Rina; Cheung, Fung Kei; Clarkson, Guy C.; Martins, Jose E. D.; Graham, Mark A.; Wills, Martin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3290 - 3294
反应条件
palladium monocarbide in methanol; water
参考文献
Pennwalt Corporation
Patent: US4766131 A1, 1988 ;
反应条件
hydrogenchloride; sodium hydroxide; sodium tetrahydroborate in methanol; water
参考文献
Pennwalt Corporation
Patent: US4766131 A1, 1988 ;
反应条件
trichlorophosphate in toluene
T=20 - 111°C; 2 h; Inert atmosphere;
参考文献
Soni, Rina; Cheung, Fung Kei; Clarkson, Guy C.; Martins, Jose E. D.; Graham, Mark A.; Wills, Martin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3290 - 3294
参考文献
Pennwalt Corporation
Patent: US4766131 A1, 1988 ;
反应条件
1: dichloromethane / 18 h / 18 - 20 °C / Inert atmosphere
2: trichlorophosphate / toluene / 2 h / 20 - 111 °C / Inert atmosphere
View Scheme
参考文献
Soni, Rina; Cheung, Fung Kei; Clarkson, Guy C.; Martins, Jose E. D.; Graham, Mark A.; Wills, Martin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3290 - 3294