1,3-二吡啶-2-基脲合成路线 (共 32 条)
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=20°C; 27 h;
参考文献
Corbin; Zimmerman; Thiessen; Hawryluk; Murray
Journal of the American Chemical Society, 2001 , vol. 123, # 43 p. 10475 - 10488
反应条件
tetra-n-butylammonium tetrafluoroborate; sodium acetate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=50°C; P=760 Torr; 5 h; Electrolysis;
参考文献
Chiarotto, Isabella; Feroci, Marta
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 7137 - 7139
反应条件
in tetrahydrofuran T=100°C; P=6000480 Torr; 72 h;
参考文献
Azad, Saleha; Kumamoto, Koji; Uegaki, Kaoru; Ichikawa, Yoshiyasu; Kotsuki, Hiyoshizo
Tetrahedron Letters, 2006 , vol. 47, # 4 p. 587 - 590
反应条件
in dimethyl sulfoxide T=80 - 90°C; 2 h;
参考文献
Ohsawa; Arai; Igeta
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 12 p. 3570 - 3575
反应条件
in decalin T=80°C; 2 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 12 p. 3570 - 3575
反应条件
selenium; oxygen; triethylamine in toluene T=140°C; 3 h; Autoclave;
参考文献
Synthesis (Germany), , vol. 45, # 10 art. no. SS-2013-F0083-OP, p. 1357 - 1363
反应条件
selenium; oxygen; triethylamine in toluene T=140°C; 3 h; Autoclave;
参考文献
Synthesis (Germany), , vol. 45, # 10 art. no. SS-2013-F0083-OP, p. 1357 - 1363
反应条件
in tert-butyl alcohol Ambient temperature;
参考文献
Venuti, Michael C.; Stephenson, Robert A.; Alvarez, Robert; Bruno, John J.; Strosberg, Arthur M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2136 - 2145
反应条件
selenium; oxygen; triethylamine in toluene T=140°C; 3 h; Autoclave;
参考文献
Synthesis (Germany), , vol. 45, # 10 art. no. SS-2013-F0083-OP, p. 1357 - 1363
反应条件
selenium; oxygen; triethylamine in toluene T=140°C; 3 h; Autoclave;
参考文献
Synthesis (Germany), , vol. 45, # 10 art. no. SS-2013-F0083-OP, p. 1357 - 1363