反-1,3-二苯基-2-丙稀-1-醇合成路线 （共 76 条）
反应条件
Zn(BH4)2(bpy) in acetonitrile T=20°C; 3 h;
参考文献
Zeynizadeh, Behzad; Yahyaei, Saiedeh
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2004 , vol. 59, # 6 p. 699 - 703
反应条件
iodine; magnesium in tetrahydrofuran 1.) reflux; 2.) 20 deg C then 22 deg C;
参考文献
Stoner, Eric J.; Cothron, Darlene A.; Balmer, Mary K.; Roden, Brian A.
Tetrahedron, 1995 , vol. 51, # 41 p. 11043 - 11062
反应条件
potassium hydroxide; SIDip*HCl; dirhodium tetraacetate in methanol 1.5 h; Heating;
参考文献
Trindade, Alexandre F.; Gois, Pedro M. P.; Veiros, Luis F.; Andre, Vania; Duarte, M. Teresa; Afonso, Carlos A. M.; Caddick, Stephen; Cloke, F. Geoffrey N.
Journal of Organic Chemistry, 2008 , vol. 73, # 11 p. 4076 - 4086
反应条件
hexadecyltrimethylammonium hydroxide; malonic acid dimethyl ester; (rac)-BINAP; bis(η3-allyl-μ-chloropalladium(II)) in water T=25°C; 1 h;
参考文献
Sinou, Denis; Rabeyrin, Cedric; Nguefack, Christelle
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 3 p. 357 - 363
反应条件
1-phenyl-1-propyne; water; bis(1,5-cyclooctadiene)nickel (0) in 1,4-dioxane T=80°C; 12 h;
参考文献
Takahashi, Go; Shirakawa, Eiji; Tsuchimoto, Teruhisa; Kawakami, Yusuke
Chemical Communications, 2005 , # 11 p. 1459 - 1461
反应条件
chromium dichloride in N,N-dimethyl-formamide T=25°C; 1 h;
参考文献
Takai, Kazuhiko; Kimura, Keizo; Kuroda, Tooru; Hiyama, Tamejiro; Nozaki, Hitosi
Tetrahedron Letters, 1983 , vol. 24, # 47 p. 5281 - 5284
反应条件
borohydride Ultra resin in methanol T=20°C; 16 h;
参考文献
Tetrahedron, , vol. 60, # 39 p. 8703 - 8709
反应条件
diethylzinc in hexane; toluene T=0°C; 0.5 h;
参考文献
Garcia, Celina; Libra, Eric R.; Carroll, Patrick J.; Walsh, Patrick J.
Journal of the American Chemical Society, 2003 , vol. 125, # 11 p. 3210 - 3211
反应条件
in tetrahydrofuran T=0 - 20°C; 16 h;
参考文献
Kelly, Brian G.; Gilheany, Declan G.
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 887 - 890
反应条件
1: With DEMS; [RhCl(PPh3)3]/Pd(OAc)2/polyammonium iodide gel in 1,4-dioxane T=60°C; 2 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran; 1,4-dioxane T=60°C; Hiyama cross-coupling reaction; 12 h; Further stages.;
参考文献
Thiot, Carine; Schmutz, Marc; Wagner, Alain; Mioskowski, Charles
Chemistry - A European Journal, 2007 , vol. 13, # 32 p. 8971 - 8978
