2-(苯基甲基)-苯并噻唑合成路线 （共 39 条）
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; 4 h;
参考文献
Zhong; Zhang; Chen
Journal of the Indian Chemical Society, 2001 , vol. 78, # 6 p. 316 - 318
反应条件
in tetrahydrofuran
T=20°C; 0.25 h;
参考文献
Harizi, Abdallah; Zantour, Hedi
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 9 p. 1883 - 1891
反应条件
pyridine; anhydrous iron chloride; sodium peroxodisulphate in dimethyl sulfoxide
T=40°C; 10 h; Inert atmosphere;
参考文献
Wang, Haibo; Wang, Lu; Shang, Jinsai; Li, Xing; Wang, Haoyuan; Gui, Jie; Lei, Aiwen
Chemical Communications, 2012 , vol. 48, # 1 p. 76 - 78
反应条件
isopropoxide ion in isopropyl alcohol
Heating;
参考文献
Florio, Saverio; Capriati, Vito; Colli, Gennara
Tetrahedron, 1997 , vol. 53, # 16 p. 5839 - 5846
反应条件
in acetic acid
1 h; Ambient temperature;
参考文献
Subhashini, N J Prameela; Hanumanthu, P
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 4 p. 427 - 429
反应条件
in toluene
24 h; Heating;
参考文献
Takahashi, Masahiko; Ohba, Masaru
Heterocycles, 1995 , vol. 41, # 3 p. 455 - 460
反应条件
FeCl3·6H2O; 1-n-butyl-3-methylimidazolium tetrafluoroborate
T=60°C; 8 h;
参考文献
Fan, Xuesen; He, Yan; Wang, Yangyang; Xue, Zaikun; Zhang, Xinying; Wang, Jianji
Tetrahedron Letters, 2011 , vol. 52, # 8 p. 899 - 902
反应条件
1: SOCl2 / 1 h / 80 °C
2: 95 percent / toluene / 0.25 h / 20 °C
View Scheme
参考文献
Rudrawar, Santosh; Kondaskar, Atul; Chakraborti, Asit K.
Synthesis, 2005 , # 15 art. no. Z05105SS, p. 2521 - 2526
反应条件
1: 46 percent / CH3SO2Cl, Et3N / 1) 0 deg C -> room temperature, 30 min, 2) reflux, 2 d
2: 20 percent / i-PrO(1-) / propan-2-ol / Heating
View Scheme
参考文献
Florio, Saverio; Capriati, Vito; Colli, Gennara
Tetrahedron, 1997 , vol. 53, # 16 p. 5839 - 5846
反应条件
1: 43 percent / 2 h / 160 - 180 °C
2: 46 percent / CH3SO2Cl, Et3N / 1) 0 deg C -> room temperature, 30 min, 2) reflux, 2 d
3: 20 percent / i-PrO(1-) / propan-2-ol / Heating
View Scheme
参考文献
Florio, Saverio; Capriati, Vito; Colli, Gennara
Tetrahedron, 1997 , vol. 53, # 16 p. 5839 - 5846
