2-(4-氯苯基)苯并噻唑合成路线 (共 73 条)
反应条件
1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate T=100°C; 0.166667 h; Microwave irradiationSealed tube;
参考文献
Wen, Xiaoan; Bakali, Jamal El; Deprez-Poulain, Rebecca; Deprez, Benoit
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2440 - 2443
反应条件
anhydrous iron chloride; Cu(OAc)2*2H2O; palladium dichloride in N,N-dimethyl-formamide T=120°C; 24 h;
参考文献
Wu, Xiang-Mei; Shen, Qiu-Xian
Letters in Organic Chemistry, 2013 , vol. 10, # 9 p. 668 - 673
反应条件
oxygen; scandium tris(trifluoromethanesulfonate) in tetrahydrofuran T=20°C; 2 h;
参考文献
Itoh, Takashi; Nagata, Kazuhiro; Ishikawa, Hiroyuki; Ohsawa, Akio
Heterocycles, 2004 , vol. 63, # 12 p. 2769 - 2783
反应条件
sodium carbonate; Pd2(PPh3)2Cl2 in toluene 3 h; Reflux;
参考文献
Lee, Mi Ae; Kwon, Hyuck Joo; Kim, Bong Ok; Kim, Sung Min; Yoon, Seung Soo
Patent: US2010/190994 A1, 2010 ;
Location in patent: Page/Page column 19-20 ;
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide T=100°C; 12 h;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
dimethyl-dichlorosilane in benzene T=40 - 45°C;
参考文献
Sonika; Meenakshi; Malhotra, Rajesh
Synthetic Communications, 2011 , vol. 41, # 1 p. 136 - 146
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
反应条件
di-μ-chlorobis [5-hydroxy-2-[1-(hydroxyimino)ethyl]phenyl]palladium(II) dimer; potassium carbonate in N,N-dimethyl acetamide T=140°C; 24 h; Inert atmosphere;
参考文献
Zhang, Guofu; Zhao, Xiaobao; Yan, Yunbing; Ding, Chengrong
European Journal of Organic Chemistry, 2012 , # 4 p. 669 - 672
反应条件
oxygen in dimethyl sulfoxide; chlorobenzene T=140°C; P=760.051 Torr; 16 h; Sealed tube;
参考文献
Liao, Yunfeng; Qi, Hongrui; Chen, Shanping; Jiang, Pengcheng; Zhou, Wang; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 23 p. 6004 - 6007
反应条件
copper diacetate; triethylamine in ethanol T=70°C; 6 h;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Wu, Xia
Organic Letters, 2013 , vol. 15, # 7 p. 1598 - 1601