1,3,5-三苯基-1,5-戊二酮合成路线 (共 55 条)
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; Barium in N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Takahashi, Hiroshi; Arai, Takayoshi; Yanagisawa, Akira
Synlett, 2006 , # 17 p. 2833 - 2835
反应条件
sodium hydroxide in ethanol 2 h; Ambient temperature;
参考文献
Yayli, Nurettin
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 6 p. 556 - 561
反应条件
1: With Me2AlNTf2 in dichloromethane T=-45°C; Addition; Michael addition; 3 h; 2: With hydrogenchloride; water in tetrahydrofuran; dichloromethane Hydrolysis;
参考文献
Marx, Andreas; Yamamoto, Hisashi
Angewandte Chemie - International Edition, 2000 , vol. 39, # 1 p. 178 - 181
反应条件
gold(III) chloride; silver hexafluoroantimonate in methanol; acetonitrile T=20°C; Inert atmosphere;
参考文献
Waldmann, Herbert; Karunakar, Galla V.; Kumar, Kamal
Organic Letters, 2008 , vol. 10, # 11 p. 2159 - 2162
反应条件
gold(III) chloride; silver hexafluoroantimonate in methanol; acetonitrile T=20°C; Inert atmosphere;
参考文献
Waldmann, Herbert; Karunakar, Galla V.; Kumar, Kamal
Organic Letters, 2008 , vol. 10, # 11 p. 2159 - 2162
反应条件
samarium (III) iodide in tetrahydrofuran T=20°C; 4 h;
参考文献
Zheng, Xingliang; Zhang, Yongmin
Journal of Chemical Research, 2004 , # 6 p. 412 - 413
反应条件
sodium hydroxide; ethanol
参考文献
Chemische Berichte, , vol. 29, p. 1492
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; Barium in N,N-dimethyl-formamide T=20°C; Michael addition; 24 h;
参考文献
Takahashi, Hiroshi; Arai, Takayoshi; Yanagisawa, Akira
Synlett, 2006 , # 17 p. 2833 - 2835
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane 6 h; Ambient temperature;
参考文献
Swamy, Vishwanath M.; Sarkar, Amitabha
Tetrahedron Letters, 1998 , vol. 39, # 10 p. 1261 - 1264
反应条件
1: With boron trifluoride diethyl etherate in toluene T=90°C; Addition; 1 h; 2: With oxalic acid Cyclization; 21 h; Heating;
参考文献
Brown, Catherine D.; Chong, J. Michael; Shen, Lixin
Tetrahedron, 1999 , vol. 55, # 50 p. 14233 - 14242