in tetrahydrofuran
under Ar; PhCH2Cl added dropwise at ambient temp. to soln. of Fe complexin THF; stirred for 12 h; evapd. to dryness under reduced pressure; washed with n-hexane;
Al'fonsov, V. A.; Nizamov, I. S.; Katsyuba, S. A.; Batyeva, E. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 6 p. 1273 - 1288,1131 - 1144
tetraphosphorus trisulfide
T=200°C; Further byproducts given;
参考文献
Nizamov, Il'yas S.; Batyeva, Elvira S.; Al'fonsov, Vladimir A.; Musin, Rashid Z.; Pudovik, Arkady N.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 55, # 1-4 p. 229 - 237
benzaldehyde
T=190 - 200°C; 1 h; in a sealed tube;
参考文献
Al'fonsov, V. A.; Nizamov, I. S.; Katsyuba, S. A.; Batyeva, E. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 6 p. 1273 - 1288,1131 - 1144
sulfuric acid in carbon disulfide
40 h; Ambient temperature;
参考文献
El-Khawaga, A. M.; El-Zohry, M. F.; Ismail, M. T.; Abdel-Wahab, A. A.; Khalaf, A. A.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 29, p. 265 - 270
