2-苯亚甲基-1-四氢萘酮合成路线 （共 24 条）
反应条件
potassium hydroxide in ethanol 24 h; Inert atmosphereSchlenk technique;
参考文献
Weemers, Jarno J. M.; Van Der Graaff, Willem N. P.; Pidko, Evgeny A.; Lutz, Martin; Mueller, Christian
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 8991 - 9004
反应条件
methanol; di-n-butyltin dimethoxide in tetrahydrofuran T=50°C; 72 h;
参考文献
Yanagisawa, Akira; Goudu, Riku; Arai, Takayoshi
Organic Letters, 2004 , vol. 6, # 23 p. 4281 - 4283
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in N,N-dimethyl-formamide T=100°C; P=30400 Torr; 28 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 118, # 25 p. 5904 - 5918
反应条件
1: 30 percent / CuI, Cl2Pd(PPh3)2, Et2NH / 24 h / 25 °C 2: 50 percent / i-Bu2AlH / hexane / 20 h / 50 °C 3: Et3N, Cl2Pd(PPh3)2 / dimethylformamide / 28 h / 100 °C / 30400 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 118, # 25 p. 5904 - 5918
反应条件
1: 50 percent / i-Bu2AlH / hexane / 20 h / 50 °C 2: Et3N, Cl2Pd(PPh3)2 / dimethylformamide / 28 h / 100 °C / 30400 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 118, # 25 p. 5904 - 5918
反应条件
pyridine hydrochloride T=220°C; 0.25 h; Yield given;
参考文献
Tetrahedron, , vol. 36, p. 1381 - 1384
反应条件
1.1: silica-supported poly-L-leucine; urea-H2O2; BEMP / tetrahydrofuran / 20 °C 1.2: diethyl ether; tetrahydrofuran / -78 °C 2.1: 40 percent / Yb(OTf)3 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Hauer, Bernhard; Bickley, Jamie F.; Massue, Julien; Pena, Paula C. A.; Roberts, Stanley M.; Skidmore, John
Canadian Journal of Chemistry, 2002 , vol. 80, # 6 p. 546 - 550
反应条件
1: 20 percent / NaBH4 / pyridine 2: 68 percent / p-toluenesulphonic acid / toluene / Heating View Scheme
参考文献
Cuppen, Th. J. H. M.; Berendsen, N.; Laarhoven, W. H.
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, # 3 p. 168 - 171
参考文献
Rapson; Shuttleworth
Journal of the Chemical Society, 1940 , p. 636,640
参考文献
Katritzky, Alan R.; El-Mowafy, Azzahra M.; Marzorati, Liliana; Patel, Ranjan C.; Thind, Sukhpal S.
Journal of Chemical Research, Miniprint, 1980 , # 9 p. 4001 - 4030
