反应条件
1: 80 percent / acetonitrile / 48 h / Heating
2: 1.) n-BuLi / 1.) THF, hexane, -20 deg C, 1.5 h, 2.) a) -78 deg C, 2 h, b) -78 deg C to 0 deg C, 3 h
3: 100 percent / H2 / 10percent Pd/C / petroleum ether / 12 h / 11250.9 Torr
4: 83 percent / Bu4NF / tetrahydrofuran
View Scheme
参考文献
Genard, S.; Patin, H.
Bulletin de la Societe Chimique de France, 1991 , # 3 p. 397 - 406
