4,4’-双(二甲氨基)偶氮苯合成路线 （共 29 条）
反应条件
hydrogenchloride; tin(ll) chloride T=60°C;
参考文献
Jacobson
Justus Liebigs Annalen der Chemie, 1922 , vol. 427, p. 219
参考文献
Jacobson
Justus Liebigs Annalen der Chemie, 1922 , vol. 427, p. 219
参考文献
Barbier; Vignon
Bulletin de la Societe Chimique de France, 1887 , vol. <2>48, p. 637
参考文献
Chemische Berichte, , vol. 16, p. 1421
Monatshefte fuer Chemie, , vol. 4, p. 292
反应条件
hydrogenchloride; sodium nitrite
durch Diazotierung und Kupplung der Diazoverbindung mit dimethylanilin;
参考文献
Nietzki
Chemische Berichte, 1885 , vol. 18, p. 1145
反应条件
1: With hydrogen; potassium hydroxide in para-xylene
T=120°C; P=760.051 Torr; 24 h;
2: With oxygen in para-xylene
T=120°C; 2 h;
参考文献
Hu, Lei; Cao, Xueqing; Shi, Linyan; Qi, Fenqiang; Guo, Zhiqiang; Lu, Jianmei; Gu, Hongwei
Organic Letters, 2011 , vol. 13, # 20 p. 5640 - 5643
反应条件
diethyl ether
T=-10°C; oder anderen Organomagnesiumverbindungen;
参考文献
Wieland; Koegl
Chemische Berichte, 1922 , vol. 55, p. 1802
Full Text Show Details
Gilman; McCracken
Journal of the American Chemical Society, 1927 , vol. 49, p. 1058
Journal of the American Chemical Society, 1929 , vol. 51, p. 825
Full Text Show Details
Wieland
Chemische Berichte, 1903 , vol. 36, p. 2319
反应条件
Lawesson's reagent in benzene
T=25°C; 2 h;
参考文献
Jorgensen, K. A.; Shabana, R.; Scheibye, S.; Lawesson, S.-O.
Bulletin des Societes Chimiques Belges, 1980 , vol. 89, # 3 p. 247 - 254
反应条件
Ru/C; sodium hydroxide in tetrahydrofuran; ethanol
T=120°C; 24 h; Microwave irradiation;
参考文献
Kim, Ju Hyun; Park, Ji Hoon; Chung, Young Keun; Park, Kang Hyun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2412 - 2418
反应条件
C6H4N2O4(1-)*K(1+) in tetrahydrofuran
T=-20°C; 1 h;
参考文献
Todres, Z. V.; Ovsepyan G. Ts.; Kosnikov, A. Yu.; Lindeman, S. V.; Struchkov, Yu. T.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 3.2 p. 522 - 527
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 3 p. 610 - 616
