2-(2-二乙氧基磷酰乙基)异吲哚-1,3-二酮合成路线 （共 9 条）
反应条件
hydrogenchloride Yield given;
参考文献
Cameron, David G.; Hudson, Harry R.; Pianka, Max
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 83, # 1-4 p. 21 - 38
反应条件
hydrogenchloride 1 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Yamauchi, Kiyoshi; Ohtsuki, Souichi; Kinoshita, Masayoshi
Journal of Organic Chemistry, 1984 , vol. 49, # 7 p. 1158 - 1163
参考文献
Neidlein, Richard; Greulich, Peter
Helvetica Chimica Acta, 1992 , vol. 75, # 8 p. 2545 - 2552
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
8 h; Heating;
参考文献
Chun; Park; Oh; Hong; Kim
Synthesis, 1994 , # 9 p. 909 - 910
反应条件
potassium carbonate in acetonitrile
48 h; Inert atmosphereReflux;
参考文献
Zhou, Liang
Journal of Chemical Research, 2012 , vol. 36, # 9 p. 512 - 515
反应条件
1: 71 percent / NEt3 / CH2Cl2 / 6 h / Heating
2: 84 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 8 h / Heating
View Scheme
参考文献
Chun; Park; Oh; Hong; Kim
Synthesis, 1994 , # 9 p. 909 - 910
反应条件
1: acetone / 16 h / Heating
2: 67.1 percent / 3 h / 180 °C
View Scheme
参考文献
Neidlein, Richard; Greulich, Peter
Helvetica Chimica Acta, 1992 , vol. 75, # 8 p. 2545 - 2552
反应条件
hydrogenchloride
1 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Yamauchi, Kiyoshi; Ohtsuki, Souichi; Kinoshita, Masayoshi
Journal of Organic Chemistry, 1984 , vol. 49, # 7 p. 1158 - 1163
反应条件
hydrazine hydrate in ethanol
a) r.t., overnight, b) reflux, 2 h;
参考文献
Neidlein, Richard; Greulich, Peter
Helvetica Chimica Acta, 1992 , vol. 75, # 8 p. 2545 - 2552
