2,4-二甲基-2-戊烯合成路线 (共 80 条)
反应条件
nickel Hydrogenation.unter hohem Druck;
参考文献
Industrial and Engineering Chemistry, , vol. 41, p. 615
反应条件
copper(II) bis(trifluoromethanesulfonate)
参考文献
Laali, Khosrow; Gerzina, Robert J.; Flajnik, Christine M.; Geric, Cynthia M.; Dombroski, Ann Marie
Helvetica Chimica Acta, 1987 , vol. 70, p. 607 - 611
反应条件
hydrogen; silica-supported dendrimer-palladium complex (G0-Pd) in methanol T=25°C; P=724.007 Torr; 1.5 h; Title compound not separated from byproducts;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 6 p. 725 - 731
反应条件
1: [i-PrPPh3](+)Br(-) With n-butyllithium in diethyl ether; pentane T=0 - 20°C; 10 h; 2: isobutyraldehyde in diethyl ether; pentane Wittig reaction; 24 h; Heating;
参考文献
Miller, Aubry K.; Hughes, Chambers C.; Kennedy-Smith, Joshua J.; Gradl, Stefan N.; Trauner, Dirk
Journal of the American Chemical Society, 2006 , vol. 128, # 51 p. 17057 - 17062
反应条件
iodine in diethyl ether 0.5 h; Heating;
参考文献
Bushby, Richard; Mann, Stephen
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2497 - 2504
反应条件
1: 1.) N2H4*H2O, 2.) I2, Et3N / 1.) ethanol, reflux, 1 h, 2.) THF, room temperature, 1 h 2: 16 percent Chromat. / methanol / 4 h / Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 105, # 23 p. 6907 - 6915
反应条件
1: HMn(CO)4 / benzene / 29 °C / other reagent and temperature 2: HMn(CO)4 / benzene / 29 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 108, # 7 p. 1689 - 1691
反应条件
aluminum oxide T=350 - 375°C;
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1651
反应条件
isopropyl alcohol; magnesium oxide T=199.9°C; Yields of byproduct given;
参考文献
Kijenski, Jacek; Glinski, Marek; Czarnecki, Jacek
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 11 p. 1695 - 1698
反应条件
triethanolamine; 2-butoxy-ethanol
参考文献
Journal of the American Chemical Society, , vol. 77, p. 3610,3613