oxonium; zinc in tetrahydrofuran T=-40°C; 48 h; study of the hydrolysis reaction of organozinc compound derived from the γ-crotonic trimethylsilyl ester; Product distribution;
参考文献
Bellassoued, M.; Gaudemar, M.; Borgi, A. El.; Baccar, B.
Journal of Organometallic Chemistry, 1985 , vol. 280, p. 165 - 172
hydrogenchloride in diethyl ether CO2 was bubbled through a cold (-78°C) soln. of compound in ether in the absence of light for 3-4 h, aq. HCl was added;;